Ferroelasticity and infrared emissivity of （Nd1－  x Ca  x ）（Al1－  x Fe  x ）O3－  x /2 （x=0-0.3）

Yue ZHANG; Yanfei WANG; Jinping DU; Fan WAN; Junsheng LI; Duan LI; Rongjun LIU

doi:10.11868/j.issn.1001-4381.2023.000145

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Journal of Materials Engineering ›› 2023, Vol. 51 ›› Issue (11) : 87-93. DOI: 10.11868/j.issn.1001-4381.2023.000145

RESEARCH ARTICLE

Ferroelasticity and infrared emissivity of （Nd_1－ _x Ca _x ）（Al_1－ _x Fe _x ）O_3－ _x _/2 （x=0-0.3）

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Abstract

Using a high temperature solid state reaction at 1600 ℃ for 6 h，（Nd_1－ _x Ca _x ）（Al_1－ _x Fe _x ）O_3－ _x _/2（x=0，0.1，0.2，0.3） was synthesized by introducing Ca²⁺ and Fe³⁺ into NdAlO₃， and spark plasma sintering （SPS） ceramic samples were used to investigate the effects of Ca²⁺ and Fe³⁺ addition on the phase composition，emissivity and ferroelasticity of NdAlO₃. The results show that a solid solution can be successfully fabricated through the high temperature solid state reaction. The doping of Ca²⁺ and Fe³⁺ in NdAlO₃ increases oxygen vacancies and slight lattice distortion occurs，emissivity of NdAlO₃ within the wavelength range of 2.5-10 μm increases the maximum to 0.9. The introduction of impurity ions makes the phase gradually transform from rhombohedral to cubic，leading to the ferroelastic domains vanish. However，the fracture toughness of ceramic samples remains at a high level.

Key words

NdAlO₃ / perovskite / ferroelastic domain / emissivity / doping

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Yue ZHANG , Yanfei WANG , Jinping DU , et al . Ferroelasticity and infrared emissivity of （Nd_1－ _x Ca _x ）（Al_1－ _x Fe _x ）O_3－ _x _/2 （x=0-0.3）[J]. Journal of Materials Engineering. 2023, 51(11): 87-93 https://doi.org/10.11868/j.issn.1001-4381.2023.000145

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