Interlayer Spacing Regulations on MoS2-Based Supercapacitors： Recent Advances and Challenges

Wu Mingyu; Ma Dongliang; Hua Qingsong; Lu Shun

doi:10.7536/PC20250605

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Prog Chem ›› 2025, Vol. 37 ›› Issue (9) : 1235-1260. DOI: 10.7536/PC20250605

Review

Interlayer Spacing Regulations on MoS₂-Based Supercapacitors： Recent Advances and Challenges

Wu Mingyu ¹ ,
Ma Dongliang ¹^,^* ,
Hua Qingsong ²^,^* ,
Lu Shun ³^,^*

Author information +

History +

Abstract

Due to its unique layered structure and excellent electrochemical properties， molybdenum disulfide （MoS₂） demonstrates significant potential for applications in the energy storage field， particularly in supercapacitors. It is widely regarded as one of the most representative transition metal dichalcogenides. MoS₂possesses a high theoretical specific capacitance， abundant edge active sites， and favorable tunability and structural diversity， which provide it with a distinct advantage in the construction of advanced electrode structures. Additionally， the anisotropic characteristics of MoS₂concerning electron and ion transport offer more dimensions for regulating its electrochemical behavior. This work will systematically review various synthesis strategies for MoS₂and its recent advancements in energy storage， with a particular focus on the mechanisms by which interlayer spacing modulation affects energy storage behavior in supercapacitor configurations. The discussion will encompass a comprehensive logical framework that spans material structure modifications， electronic configuration evolution， and enhancements in macroscopic device performance. This review aims to provide theoretical support and practical guidance for the application of MoS₂in the next generation of high-performance energy storage devices.

Contents

1 Introduction

2 Overview of MoS₂ as a fundamental electrode material for supercapacitors

3 Synthesis strategies of MoS₂

3.1 “Bottom-up” synthesis of MoS₂

3.2 “Top-down” synthesis of MoS₂

4 Strategy of modulating MoS₂ interlayer spacing and the effects on electrochemical properties

4.1 Interlayer agent induces interlayer spacing expansion

4.2 3D structure construction

4.3 Defect engineering

4.4 Other methods to regulate the interlayer spacing of MoS₂

4.5 Theoretical understanding

5 Summary and outlook

Key words

supercapacitor / two-dimensional materials / MoS₂ / interlayer spacing / electrochemical property

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Wu Mingyu , Ma Dongliang , Hua Qingsong , et al. Interlayer Spacing Regulations on MoS₂-Based Supercapacitors： Recent Advances and Challenges[J]. Progress in Chemistry. 2025, 37(9): 1235-1260 https://doi.org/10.7536/PC20250605

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Funding

The Xinjiang Uygur Automomous Region Science and Technology Plan Project-Key R&D Special Project(2022B02051)

The Semiconductor physics and micro and nano devices Tianshan Innovation team(2023D14001)

The Tianshan Talent Training Project-Xinjiang Science and Technology Innovation Team Program(2023TSYCTD0012)

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